The products of ecological textile have represented nowadays the new trend ofglobal consumption and production of textile while become an important means for some countries toutilize 'green barrier' as a limit...The products of ecological textile have represented nowadays the new trend ofglobal consumption and production of textile while become an important means for some countries toutilize 'green barrier' as a limitation of import of textile products. Following the entrance ofChina into the WTO, the position of 'green barrier' becomes significantly important in the trade oftextile products. As China is a big country of textile production, speeding up the research onstandards for products of ecological textile, countering the latest situation appearing ininternational trade of textile, to take as quickly as possible responsive measures is a very urgentproblem in port, to enhancing the ability of international market competition and to promoting thestable development of foreign oriented economy.展开更多
A high-performance liquid chromatography （HPLC） system was used in the reversed phase mode for the determination ofbenzalkonium chloride （BKC） in azithromycin viscous ophthalmic drops. A Venusil-XBP（L）-C18 （150...A high-performance liquid chromatography （HPLC） system was used in the reversed phase mode for the determination ofbenzalkonium chloride （BKC） in azithromycin viscous ophthalmic drops. A Venusil-XBP（L）-C18 （150 mm×4.6 mm, 5 gm） column was used at 50℃. The mobile phase consisted of a mixture of methanol-potassium phosphate （16：5, v/v）. Two sample preparation methods were compared. The results suggested that, compared with an extraction procedure, a deproteinization procedure was much quicker and more convenient. Using the deproteinization procedure for sample preparation, calibration curves were linear in the range 5.0-50μg/ml. The within-day and inter-day coefficients of variation were less than 10%. The average recoveries were determined as 96.70%, 98.52%, and 97.96% at concentrations of 10.0, 30.0, and 50.0 μg/ml, respectively. Variability in precision did not exceed 5%. In conclusion, this HPLC method using a simple sample treatment procedure appears suitable for monitoring BKC content in azithromycin viscous ophthalmic drops.展开更多
文摘The products of ecological textile have represented nowadays the new trend ofglobal consumption and production of textile while become an important means for some countries toutilize 'green barrier' as a limitation of import of textile products. Following the entrance ofChina into the WTO, the position of 'green barrier' becomes significantly important in the trade oftextile products. As China is a big country of textile production, speeding up the research onstandards for products of ecological textile, countering the latest situation appearing ininternational trade of textile, to take as quickly as possible responsive measures is a very urgentproblem in port, to enhancing the ability of international market competition and to promoting thestable development of foreign oriented economy.
基金Project (No. 2008BAI55B03) supported by the Key Project of the National Science and Technology Pillar Program, China
文摘A high-performance liquid chromatography （HPLC） system was used in the reversed phase mode for the determination ofbenzalkonium chloride （BKC） in azithromycin viscous ophthalmic drops. A Venusil-XBP（L）-C18 （150 mm×4.6 mm, 5 gm） column was used at 50℃. The mobile phase consisted of a mixture of methanol-potassium phosphate （16：5, v/v）. Two sample preparation methods were compared. The results suggested that, compared with an extraction procedure, a deproteinization procedure was much quicker and more convenient. Using the deproteinization procedure for sample preparation, calibration curves were linear in the range 5.0-50μg/ml. The within-day and inter-day coefficients of variation were less than 10%. The average recoveries were determined as 96.70%, 98.52%, and 97.96% at concentrations of 10.0, 30.0, and 50.0 μg/ml, respectively. Variability in precision did not exceed 5%. In conclusion, this HPLC method using a simple sample treatment procedure appears suitable for monitoring BKC content in azithromycin viscous ophthalmic drops.
