A new sulfanilamide Schiff-base compound N,N -（p-phenyl sulfanilamide）-5,6-dimethoxy-pyrimidine-（2-hydroxyl benzene） methylidene has been synthesized by the condensation of equimolar salicylaldehyde and 4-（p-amin...A new sulfanilamide Schiff-base compound N,N -（p-phenyl sulfanilamide）-5,6-dimethoxy-pyrimidine-（2-hydroxyl benzene） methylidene has been synthesized by the condensation of equimolar salicylaldehyde and 4-（p-amino phenyl sulfanilamide）-5,6-dimethoxy-pyrimidine in an anhydrous ethanol solution.The compound was characterized by elemental analysis,IR spectra,and single-crystal X-ray diffraction.The crystal belongs to the monoclinic system,space group P21/c with a=19.0425（11）,b=11.1914（6）,c=9.0075（5）,β=93.9650（10）°,Z= 4, V= 1915.01（18） A3,Dc = 1.437 g/cm^3, Mr = 414.43, λ（MoKa） = 0.71073 A,μ= 2.09 mm^-1, F（000） = 864, R = 0.0385 and wR = 0.1224.展开更多
基金supported by the Natural Science Foundation of Jiangxi Province (2008GZH0064)the Sustentation Fund of Education Department from Jiangxi Province (GJJ08275)
文摘A new sulfanilamide Schiff-base compound N,N -（p-phenyl sulfanilamide）-5,6-dimethoxy-pyrimidine-（2-hydroxyl benzene） methylidene has been synthesized by the condensation of equimolar salicylaldehyde and 4-（p-amino phenyl sulfanilamide）-5,6-dimethoxy-pyrimidine in an anhydrous ethanol solution.The compound was characterized by elemental analysis,IR spectra,and single-crystal X-ray diffraction.The crystal belongs to the monoclinic system,space group P21/c with a=19.0425（11）,b=11.1914（6）,c=9.0075（5）,β=93.9650（10）°,Z= 4, V= 1915.01（18） A3,Dc = 1.437 g/cm^3, Mr = 414.43, λ（MoKa） = 0.71073 A,μ= 2.09 mm^-1, F（000） = 864, R = 0.0385 and wR = 0.1224.
