To enhance the fracture toughness of pressureless-sintered SiC ceramic, graphene was introduced as an additive. The effects of graphene contents on the fracture toughness, bending strength, micro-hardness, phase compo...To enhance the fracture toughness of pressureless-sintered SiC ceramic, graphene was introduced as an additive. The effects of graphene contents on the fracture toughness, bending strength, micro-hardness, phase compositions, and microstructure evolutions of the SiC ceramics were investigated in detail by scanning electron microscopy, energy dispersive X-ray spectroscopy, and metallographic microscopy. The fracture toughness, bending strength and micro-hardness increased initially, and then decreased with the graphene content increasing from 0 to 5.0 wt%. The highest fracture toughness of 5.65 MPa m1/2 was obtained for sample with 1.0 wt% graphene sintered at 2130 ℃ for 1 h in At, which was about 22.6% higher than that of SiC sample without graphene. In addition, the highest bending strength and microhardness of 434.14 MPa and 29.21 GPa corresponded to the SiC samples with graphene content of 0.5 wt% and 2.0 wt%, respectively.展开更多
文摘To enhance the fracture toughness of pressureless-sintered SiC ceramic, graphene was introduced as an additive. The effects of graphene contents on the fracture toughness, bending strength, micro-hardness, phase compositions, and microstructure evolutions of the SiC ceramics were investigated in detail by scanning electron microscopy, energy dispersive X-ray spectroscopy, and metallographic microscopy. The fracture toughness, bending strength and micro-hardness increased initially, and then decreased with the graphene content increasing from 0 to 5.0 wt%. The highest fracture toughness of 5.65 MPa m1/2 was obtained for sample with 1.0 wt% graphene sintered at 2130 ℃ for 1 h in At, which was about 22.6% higher than that of SiC sample without graphene. In addition, the highest bending strength and microhardness of 434.14 MPa and 29.21 GPa corresponded to the SiC samples with graphene content of 0.5 wt% and 2.0 wt%, respectively.
