Static recrystallization(SRX)behaviors and corresponding recrystallization mechanisms of 7Mo super-austenitic stainless steel were studied under different deformation conditions.The order of influence of deformation p...Static recrystallization(SRX)behaviors and corresponding recrystallization mechanisms of 7Mo super-austenitic stainless steel were studied under different deformation conditions.The order of influence of deformation parameters on static recrystallization behaviors,from high to low,is followed by temperature,first-stage strain and strain rate.Meanwhile,the effect of holding time on static recrystallization behaviors is significantly controlled by temperature.In addition,with the increase in temperature from 1000 to 1200°C,the static recrystallization mechanism evolves from discontinuous static recrystallization and continuous static recrystallization(cSRX)to metadynamic recrystallization and cSRX,and finally to cSRX.The cSRX exists at all temperatures.This is because high stacking fault energy(56 mJ m−2)promotes the movement of dislocations,making the deformation mechanism of this steel is dominated by planar slip of dislocation.Large undissolved sigma precipitates promote static recrystallization through particle-stimulated nucleation.However,small strain-induced precipitates at grain boundaries hinder the nucleation of conventional SRX and the growth of recrystallized grains,while the hindering effect decreases with the increase in temperature.展开更多
The thermal conductivity of diamond particles reinforced copper matrix composite as an attractive thermal management material is significantly lowered by the non-wetting heterointerface.The paper investigates the heat...The thermal conductivity of diamond particles reinforced copper matrix composite as an attractive thermal management material is significantly lowered by the non-wetting heterointerface.The paper investigates the heat transport behavior between a 200-nm Cu layer and a single-crystalline diamond substrate inserted by a chromium(Cr)interlayer having a series of thicknesses from 150 nm down to 5 nm.The purpose is to detect the impact of the modifying interlayer thickness on the interfacial thermal conductance(h)between Cu and diamond.The time-domain thermoreflectance measurements suggest that the introduction of Cr interlayer dramatically improves the h between Cu and diamond owing to the enhanced interfacial adhesion and bridged dissimilar phonon states between Cu and diamond.The h value exhibits a decreasing trend as the Cr interlayer becomes thicker because of the increase in thermal resistance of Cr interlayer.The high h values are observed for the Cr interlayer thicknesses below 21 nm since phononic transport channel dominates the thermal conduction in the ultrathin Cr layer.The findings provide a way to tune the thermal conduction across the metal/nonmetal heterogeneous interface,which plays a pivotal role in designing materials and devices for thermal management applications.展开更多
With the miniaturization and integration of microelectronic components,power density of electronic devices such as integrated circuits,light emitting diodes(LEDs),and semiconductor lasers increases dramatically[1].Tra...With the miniaturization and integration of microelectronic components,power density of electronic devices such as integrated circuits,light emitting diodes(LEDs),and semiconductor lasers increases dramatically[1].Traditional thermal management materials are difficult to maintain the safety and reliability of the highpower devices.展开更多
In the present study,the effect of grit blasting and subsequent heat treatment on the stress rupture properties of a thirdgeneration nickel-based single-crystal superalloy SGX3 sheet was studied.It was found that the ...In the present study,the effect of grit blasting and subsequent heat treatment on the stress rupture properties of a thirdgeneration nickel-based single-crystal superalloy SGX3 sheet was studied.It was found that the stress rupture life of alloy SGX3 sheet at 980℃/250 MPa was reduced by about 60%by only vacuum heat treatment at 1100℃ for 200 h and further reduced by 20%and 70%respectively with grit blasting of 0.3 MPa/1 min and 0.5 MPa/2 min before heat treatment.The microstructure analysis results indicated that the degradation of stress rupture life of alloy SGX3 sheet by vacuum heat treatment was mainly attributed to the variation ofγ/γ′microstructure,i.e.,the decrease inγ′volume fraction and the coarsening ofγ′precipitates.Furthermore,such degradation by grit blasting and subsequent vacuum heat treatment should be attributed to the formation of cellular recrystallization with different thicknesses at the surface of alloy SGX3 sheet,which not only acts as the vulnerable site for cracks to initiate and propagate but also reduces the effective loading area.展开更多
基金supported by National Natural Science Foundation of China(No.U1810207)the Innovation Pilot Project for Fusion of Science,Education and Industry(International Cooperation)from Qilu University of Technology(No.2020KJC-GH03).
文摘Static recrystallization(SRX)behaviors and corresponding recrystallization mechanisms of 7Mo super-austenitic stainless steel were studied under different deformation conditions.The order of influence of deformation parameters on static recrystallization behaviors,from high to low,is followed by temperature,first-stage strain and strain rate.Meanwhile,the effect of holding time on static recrystallization behaviors is significantly controlled by temperature.In addition,with the increase in temperature from 1000 to 1200°C,the static recrystallization mechanism evolves from discontinuous static recrystallization and continuous static recrystallization(cSRX)to metadynamic recrystallization and cSRX,and finally to cSRX.The cSRX exists at all temperatures.This is because high stacking fault energy(56 mJ m−2)promotes the movement of dislocations,making the deformation mechanism of this steel is dominated by planar slip of dislocation.Large undissolved sigma precipitates promote static recrystallization through particle-stimulated nucleation.However,small strain-induced precipitates at grain boundaries hinder the nucleation of conventional SRX and the growth of recrystallized grains,while the hindering effect decreases with the increase in temperature.
基金financially supported by the National Natural Science Foundation of China (Nos. 51871014, 51571015)the National Youth Science Foundation, China (No. 51606193)
文摘The thermal conductivity of diamond particles reinforced copper matrix composite as an attractive thermal management material is significantly lowered by the non-wetting heterointerface.The paper investigates the heat transport behavior between a 200-nm Cu layer and a single-crystalline diamond substrate inserted by a chromium(Cr)interlayer having a series of thicknesses from 150 nm down to 5 nm.The purpose is to detect the impact of the modifying interlayer thickness on the interfacial thermal conductance(h)between Cu and diamond.The time-domain thermoreflectance measurements suggest that the introduction of Cr interlayer dramatically improves the h between Cu and diamond owing to the enhanced interfacial adhesion and bridged dissimilar phonon states between Cu and diamond.The h value exhibits a decreasing trend as the Cr interlayer becomes thicker because of the increase in thermal resistance of Cr interlayer.The high h values are observed for the Cr interlayer thicknesses below 21 nm since phononic transport channel dominates the thermal conduction in the ultrathin Cr layer.The findings provide a way to tune the thermal conduction across the metal/nonmetal heterogeneous interface,which plays a pivotal role in designing materials and devices for thermal management applications.
基金financially supported by the National Natural Science Foundation of China(No.51871014)the Superior Discipline Talent Team Support Plan in Universities of Shandong Province,China。
文摘With the miniaturization and integration of microelectronic components,power density of electronic devices such as integrated circuits,light emitting diodes(LEDs),and semiconductor lasers increases dramatically[1].Traditional thermal management materials are difficult to maintain the safety and reliability of the highpower devices.
基金financially supported by the National Key Research and Development Program of China(Grant No.2016YFB0701403)the National Natural Science Foundation of China(Grant No.91860201)。
文摘In the present study,the effect of grit blasting and subsequent heat treatment on the stress rupture properties of a thirdgeneration nickel-based single-crystal superalloy SGX3 sheet was studied.It was found that the stress rupture life of alloy SGX3 sheet at 980℃/250 MPa was reduced by about 60%by only vacuum heat treatment at 1100℃ for 200 h and further reduced by 20%and 70%respectively with grit blasting of 0.3 MPa/1 min and 0.5 MPa/2 min before heat treatment.The microstructure analysis results indicated that the degradation of stress rupture life of alloy SGX3 sheet by vacuum heat treatment was mainly attributed to the variation ofγ/γ′microstructure,i.e.,the decrease inγ′volume fraction and the coarsening ofγ′precipitates.Furthermore,such degradation by grit blasting and subsequent vacuum heat treatment should be attributed to the formation of cellular recrystallization with different thicknesses at the surface of alloy SGX3 sheet,which not only acts as the vulnerable site for cracks to initiate and propagate but also reduces the effective loading area.