In current research,many researchers propose analytical expressions for calculating the packing structure of spherical particles such as DN Model,Compact Model and NLS criterion et al.However,there is still a question...In current research,many researchers propose analytical expressions for calculating the packing structure of spherical particles such as DN Model,Compact Model and NLS criterion et al.However,there is still a question that has not been well explained yet.That is:What is the core factors affecting the thermal conductivity of particles?In this paper,based on the coupled discrete element-finite difference(DE-FD)method and spherical aluminum powder,the relationship between the parameters and the thermal conductivity of the powder(ETC_(p))is studied.It is found that the key factor that can described the change trend of ETC_(p) more accurately is not the materials of the powder but the average contact area between particles(a_(ave))which also have a close nonlinear relationship with the average particle size d_(50).Based on this results,the expression for calculating the ETC_(p) of the sphere metal powder is successfully reduced to only one main parameter d_(50)and an efficient calculation model is proposed which can applicate both in room and high temperature and the corresponding error is less than 20.9%in room temperature.Therefore,in this study,based on the core factors analyzation,a fast calculation model of ETC_(p) is proposed,which has a certain guiding significance in the field of thermal field simulation.展开更多
Improvement of fabrication efficiency and part performance was the main challenge for the large-scale powder bed fusion(PBF)process.In this study,a dynamic monitoring and feedback system of powder bed temperature fiel...Improvement of fabrication efficiency and part performance was the main challenge for the large-scale powder bed fusion(PBF)process.In this study,a dynamic monitoring and feedback system of powder bed temperature field using an infrared thermal imager has been established and integrated into a four-laser PBF equipment with a working area of 2000 mm×2000 mm.The heat-affected zone(HAZ)temperature field has been controlled by adjusting the scanning speed dynamically.Simultaneously,the relationship among spot size,HAZ temperature,and part performance has been established.The fluctuation of the HAZ temperature in four-laser scanning areas was decreased from 30.85℃to 17.41℃.Thus,the consistency of the sintering performance of the produced large component has been improved.Based on the controllable temperature field,a dynamically adjusting strategy for laser spot size was proposed,by which the fabrication efficiency was improved up to 65.38%.The current research results were of great significance to the further industrial applications of large-scale PBF equipment.展开更多
A novel metal matrix composite freeform fabrication approach,fiber traction printing(FTP),is demonstrated through controlling the wetting behavior between fibers and the matrix.This process utilizes the fiber bundle t...A novel metal matrix composite freeform fabrication approach,fiber traction printing(FTP),is demonstrated through controlling the wetting behavior between fibers and the matrix.This process utilizes the fiber bundle to control the cross-sectional shape of the liquid metal,shaping it from circular to rectangular which is more precise.The FTP process could resolve manufacturing difficulties in the complex structure of continuous fiber reinforced metal matrix composites.The printing of the first layer monofilament is discussed in detail,and the effects of the fibrous coating thickness on the mechanical properties and microstructures of the composite are also investigated in this paper.The composite material prepared by the FTP process has a tensile strength of 235.2 MPa,which is close to that of composites fabricated by conventional processes.The complex structures are printed to demonstrate the advantages and innovations of this approach.Moreover,the FTP method is suited to other material systems with good wettability,such as modified carbon fiber,surfactants,and aluminum alloys.展开更多
Stray grains,the most serious casting defect,mainly occur in the platform because of the abrupt transition of the cross-section in the directional solidification of superalloy single-crystal blades.A new mould baffle ...Stray grains,the most serious casting defect,mainly occur in the platform because of the abrupt transition of the cross-section in the directional solidification of superalloy single-crystal blades.A new mould baffle technology based on 3D printing and gelcasting is proposed herein to reduce the formation of stray grains in the platform.The influence of the proposed mould baffle technology on the temperature field in the platform during solidification was investigated by simulation and experiment.The numerical simulation results indicate that the proposed mould baffle technology can effectively hinder the radiation and heat dissipation at the platform extremities,and therefore,reduce undercooling in the platform and the formation of stray grains during directional solidification.Casting trials of a hollow turbine blade were conducted using CMSX-4 superalloy.The trial results demonstrate the potential of the proposed approach for manufacturing single-crystal superalloy blades.展开更多
Cast molding process has provided a reliable, simple and cost-effective way to fabricate micro structures since decades ago. In order to obtain structures with fine, dense and deep nano-size features by cast molding, ...Cast molding process has provided a reliable, simple and cost-effective way to fabricate micro structures since decades ago. In order to obtain structures with fine, dense and deep nano-size features by cast molding, it is necessary to study the forming mechanism in the process. In this paper, based on major steps of cast molding, filling models of liquid are established and solved; and the forming mechanism of liquid is revealed. Moreover, the scale effect between the liquid and the cavity on the filling velocity of liquid is studied.It is also interesting to find out that the wettability of liquid on the cavity may be changed from wetting to dewetting depends on the pressure difference. Finally, we experimentally verify some of our modeling results on the flowing and filling state of the liquid during the cast molding process.展开更多
High-entropy alloys(HEAs)are considered alternatives to traditional structural materials because of their superior mechanical,physical,and chemical properties.However,alloy composition combinations are too numerous to...High-entropy alloys(HEAs)are considered alternatives to traditional structural materials because of their superior mechanical,physical,and chemical properties.However,alloy composition combinations are too numerous to explore.Finding a rapid synthesis method to accelerate the development of HEA bulks is imperative.Existing in situ synthesis methods based on additive manufacturing are insufficient for efficiently controlling the uniformity and accuracy of components.In this work,laser powder bed fusion(L-PBF)is adopted for the in situ synthesis of equiatomic CoCrFeMnNi HEA from elemental powder mixtures.High composition accuracy is achieved in parallel with ensuring internal density.The L-PBF-based process parameters are optimized;and two different methods,namely,a multi-melting process and homogenization heat treatment,are adopted to address the problem of incompletely melted Cr particles in the single-melted samples.X-ray diffraction indicates that HEA microstructure can be obtained from elemental powders via L-PBF.In the triple-melted samples,a strong crystallographic texture can be observed through electron backscatter diffraction,with a maximum polar density of 9.92 and a high ultimate tensile strength(UTS)of(735.3±14.1)MPa.The homogenization heat-treated samples appear more like coarse equiaxed grains,with a UTS of(650.8±16.1)MPa and an elongation of(40.2%±1.3%).Cellular substructures are also observed in the triple-melted samples,but not in the homogenization heat-treated samples.The differences in mechanical properties primarily originate from the changes in strengthening mechanism.The even and flat fractographic morphologies of the homogenization heat-treated samples represent a more uniform internal microstructure that is different from the complex morphologies of the triple-melted samples.Relative to the multi-melted samples,the homogenization heat-treated samples exhibit better processability,with a smaller composition deviation,i.e.,≤0.32 at.%.The two methods presented in this study are expected to have considerable potential for developing HEAs with high composition accuracy and composition flexibility.展开更多
This study aims to optimize the uniformity of the temperature field during sintering to improve part performance.A temperature-field monitoring system is established based on an infrared thermal imager and the tempera...This study aims to optimize the uniformity of the temperature field during sintering to improve part performance.A temperature-field monitoring system is established based on an infrared thermal imager and the temperature field data obtained during the sintering of a part can be measured in real time.The relationship among the sintering temperature field,sintering process parameters,and part performance is established experimentally.Subsequently,a temperature field monitoring and analysis system is constructed,and various sintering temperature-field control strategies are established for various part sizes.Finally,a dynamic control strategy for controlling the temperature field during sintering is proposed,experimentally validated,and fully integrated into a developed powder bed fusion(PBF)equipment.For eight-shaped standard parts,the range of sintering temperature field is optimized from 44.1℃to 19.7℃,whereas the tensile strength of the parts increased by 15.4%.For large-size H parts,localized over burning is eliminated and the final quality of the part is optimized.This strategy is critical for the optimization of the PBF process for large-sized parts,in particular in the large-sized die manufacturing industry,which offers promise in the optimization of part performance.展开更多
The changes of the wettability of the solid surfaces have attracted massive attention due to their important practical implications in numerous fields. As a new subject, the research on the wettability under the diffe...The changes of the wettability of the solid surfaces have attracted massive attention due to their important practical implications in numerous fields. As a new subject, the research on the wettability under the different environments is still in its early stage. So the fundamental research must be performed for the practical applications under different environments. However, it is seldom that the comprehensive wettability of a surface in air, in water and in oil has been reported. In this paper, the authors investigated the wettability of the stainless steel mesh coated with polyurethane in the above three different environments. The surface of the uncoated mesh was found to be hydrophobic in air, but the surface of the coated mesh was superhydrophilic in air. More interestingly, the surfaces of the coated meshes were superoleophilic in water and superhydrophobic in oil. Due to the coated meshes with these wettabilities were fabricated via a facile two-step method, the presented method may be adopted for large-scale industrial production, in various fields, such as icing prevention or the oil-field industry.展开更多
Multi-laser powder bed fusion(ML-PBF)adopts multiple laser-scanner systems to increase the build envelope and build speed,but its calibration is an iterative and time-consuming process.In particular,multiple large-sca...Multi-laser powder bed fusion(ML-PBF)adopts multiple laser-scanner systems to increase the build envelope and build speed,but its calibration is an iterative and time-consuming process.In particular,multiple large-scale scan fields have a complex distortion in the overlap area,challenging the calibration process.In this study,owing to the enormous workload and alignment problems in the calibration of multiple scan fields,a novel calibration system is designed in this study to realize in situ auto-detection of numerous laser spots in the build chamber to ensure high efficiency and accuracy.Moreover,because the detectable area could not cover the entire build area and the detection data still contained errors,a virtual laser-scanner system was established by identifying the assembly defects and galvo nonlinearities of the ML-PBF system from the detection data,which served as the system's controller to improve calibration accuracy.The multi-field alignment error was less than 0.012%,which could avoid the intersection and separation of scan paths in multi-laser scanning and therefore meet the requirements for high-precision ML-PBF.Finally,the reliability of the method was verified theoretically using principal component analysis.展开更多
基金Supported by National Natural Science Foundation of China (Grant No.51975459)Shaanxi Provincial Natural Science Foundation of China (Grant No.2017JM5046)。
文摘In current research,many researchers propose analytical expressions for calculating the packing structure of spherical particles such as DN Model,Compact Model and NLS criterion et al.However,there is still a question that has not been well explained yet.That is:What is the core factors affecting the thermal conductivity of particles?In this paper,based on the coupled discrete element-finite difference(DE-FD)method and spherical aluminum powder,the relationship between the parameters and the thermal conductivity of the powder(ETC_(p))is studied.It is found that the key factor that can described the change trend of ETC_(p) more accurately is not the materials of the powder but the average contact area between particles(a_(ave))which also have a close nonlinear relationship with the average particle size d_(50).Based on this results,the expression for calculating the ETC_(p) of the sphere metal powder is successfully reduced to only one main parameter d_(50)and an efficient calculation model is proposed which can applicate both in room and high temperature and the corresponding error is less than 20.9%in room temperature.Therefore,in this study,based on the core factors analyzation,a fast calculation model of ETC_(p) is proposed,which has a certain guiding significance in the field of thermal field simulation.
基金Supported by National High Technology Research and Development Program of China(863 Program,Grant No.2015AA042503)K.C.Wong Education Foundation.
文摘Improvement of fabrication efficiency and part performance was the main challenge for the large-scale powder bed fusion(PBF)process.In this study,a dynamic monitoring and feedback system of powder bed temperature field using an infrared thermal imager has been established and integrated into a four-laser PBF equipment with a working area of 2000 mm×2000 mm.The heat-affected zone(HAZ)temperature field has been controlled by adjusting the scanning speed dynamically.Simultaneously,the relationship among spot size,HAZ temperature,and part performance has been established.The fluctuation of the HAZ temperature in four-laser scanning areas was decreased from 30.85℃to 17.41℃.Thus,the consistency of the sintering performance of the produced large component has been improved.Based on the controllable temperature field,a dynamically adjusting strategy for laser spot size was proposed,by which the fabrication efficiency was improved up to 65.38%.The current research results were of great significance to the further industrial applications of large-scale PBF equipment.
基金Supported by National Key R&D Program of China(Grant Nos.2017YFB1103400,2016YFB1100902)National Natural Science Foundation of China(Grant No.51575430,51811530107)The Youth Innovation Team of Shaanxi Universities.
文摘A novel metal matrix composite freeform fabrication approach,fiber traction printing(FTP),is demonstrated through controlling the wetting behavior between fibers and the matrix.This process utilizes the fiber bundle to control the cross-sectional shape of the liquid metal,shaping it from circular to rectangular which is more precise.The FTP process could resolve manufacturing difficulties in the complex structure of continuous fiber reinforced metal matrix composites.The printing of the first layer monofilament is discussed in detail,and the effects of the fibrous coating thickness on the mechanical properties and microstructures of the composite are also investigated in this paper.The composite material prepared by the FTP process has a tensile strength of 235.2 MPa,which is close to that of composites fabricated by conventional processes.The complex structures are printed to demonstrate the advantages and innovations of this approach.Moreover,the FTP method is suited to other material systems with good wettability,such as modified carbon fiber,surfactants,and aluminum alloys.
基金the Industry-University Research Cooperation Project of Aero Engine Corporation of China(Grant No.HFZL2019CXY023)the National Science and Technology Major Project(Grant No.2017-Ⅶ-0008-0101)。
文摘Stray grains,the most serious casting defect,mainly occur in the platform because of the abrupt transition of the cross-section in the directional solidification of superalloy single-crystal blades.A new mould baffle technology based on 3D printing and gelcasting is proposed herein to reduce the formation of stray grains in the platform.The influence of the proposed mould baffle technology on the temperature field in the platform during solidification was investigated by simulation and experiment.The numerical simulation results indicate that the proposed mould baffle technology can effectively hinder the radiation and heat dissipation at the platform extremities,and therefore,reduce undercooling in the platform and the formation of stray grains during directional solidification.Casting trials of a hollow turbine blade were conducted using CMSX-4 superalloy.The trial results demonstrate the potential of the proposed approach for manufacturing single-crystal superalloy blades.
基金financially supported by NSFC under Grant No. 90923040China’s National "973" Program under Grant No. 2009CB724202
文摘Cast molding process has provided a reliable, simple and cost-effective way to fabricate micro structures since decades ago. In order to obtain structures with fine, dense and deep nano-size features by cast molding, it is necessary to study the forming mechanism in the process. In this paper, based on major steps of cast molding, filling models of liquid are established and solved; and the forming mechanism of liquid is revealed. Moreover, the scale effect between the liquid and the cavity on the filling velocity of liquid is studied.It is also interesting to find out that the wettability of liquid on the cavity may be changed from wetting to dewetting depends on the pressure difference. Finally, we experimentally verify some of our modeling results on the flowing and filling state of the liquid during the cast molding process.
文摘High-entropy alloys(HEAs)are considered alternatives to traditional structural materials because of their superior mechanical,physical,and chemical properties.However,alloy composition combinations are too numerous to explore.Finding a rapid synthesis method to accelerate the development of HEA bulks is imperative.Existing in situ synthesis methods based on additive manufacturing are insufficient for efficiently controlling the uniformity and accuracy of components.In this work,laser powder bed fusion(L-PBF)is adopted for the in situ synthesis of equiatomic CoCrFeMnNi HEA from elemental powder mixtures.High composition accuracy is achieved in parallel with ensuring internal density.The L-PBF-based process parameters are optimized;and two different methods,namely,a multi-melting process and homogenization heat treatment,are adopted to address the problem of incompletely melted Cr particles in the single-melted samples.X-ray diffraction indicates that HEA microstructure can be obtained from elemental powders via L-PBF.In the triple-melted samples,a strong crystallographic texture can be observed through electron backscatter diffraction,with a maximum polar density of 9.92 and a high ultimate tensile strength(UTS)of(735.3±14.1)MPa.The homogenization heat-treated samples appear more like coarse equiaxed grains,with a UTS of(650.8±16.1)MPa and an elongation of(40.2%±1.3%).Cellular substructures are also observed in the triple-melted samples,but not in the homogenization heat-treated samples.The differences in mechanical properties primarily originate from the changes in strengthening mechanism.The even and flat fractographic morphologies of the homogenization heat-treated samples represent a more uniform internal microstructure that is different from the complex morphologies of the triple-melted samples.Relative to the multi-melted samples,the homogenization heat-treated samples exhibit better processability,with a smaller composition deviation,i.e.,≤0.32 at.%.The two methods presented in this study are expected to have considerable potential for developing HEAs with high composition accuracy and composition flexibility.
基金This work is supported by the National High Technology Research and Development Program of China(863 Program)(Grant No.2015AA042503).
文摘This study aims to optimize the uniformity of the temperature field during sintering to improve part performance.A temperature-field monitoring system is established based on an infrared thermal imager and the temperature field data obtained during the sintering of a part can be measured in real time.The relationship among the sintering temperature field,sintering process parameters,and part performance is established experimentally.Subsequently,a temperature field monitoring and analysis system is constructed,and various sintering temperature-field control strategies are established for various part sizes.Finally,a dynamic control strategy for controlling the temperature field during sintering is proposed,experimentally validated,and fully integrated into a developed powder bed fusion(PBF)equipment.For eight-shaped standard parts,the range of sintering temperature field is optimized from 44.1℃to 19.7℃,whereas the tensile strength of the parts increased by 15.4%.For large-size H parts,localized over burning is eliminated and the final quality of the part is optimized.This strategy is critical for the optimization of the PBF process for large-sized parts,in particular in the large-sized die manufacturing industry,which offers promise in the optimization of part performance.
基金supported by the National Natural Science Foundation of China(Grant Nos.51475353,51375361&51475352)the Tribology Science Fund of the State Key Laboratory of Tribology(Grant No.SKLTKF14A02)+1 种基金the Natural Science Basic Research Program of Shaanxi Province(Grant No.2016JM5004)the Key Laboratory of the Shaanxi Provincial Department of Education(Grant No.16JS057)
文摘The changes of the wettability of the solid surfaces have attracted massive attention due to their important practical implications in numerous fields. As a new subject, the research on the wettability under the different environments is still in its early stage. So the fundamental research must be performed for the practical applications under different environments. However, it is seldom that the comprehensive wettability of a surface in air, in water and in oil has been reported. In this paper, the authors investigated the wettability of the stainless steel mesh coated with polyurethane in the above three different environments. The surface of the uncoated mesh was found to be hydrophobic in air, but the surface of the coated mesh was superhydrophilic in air. More interestingly, the surfaces of the coated meshes were superoleophilic in water and superhydrophobic in oil. Due to the coated meshes with these wettabilities were fabricated via a facile two-step method, the presented method may be adopted for large-scale industrial production, in various fields, such as icing prevention or the oil-field industry.
基金This study was supported by the National High Technology Research and Development Program of China(863 Program)(Grant No.2015AA042503)the K.C.Wong Education Foundation.
文摘Multi-laser powder bed fusion(ML-PBF)adopts multiple laser-scanner systems to increase the build envelope and build speed,but its calibration is an iterative and time-consuming process.In particular,multiple large-scale scan fields have a complex distortion in the overlap area,challenging the calibration process.In this study,owing to the enormous workload and alignment problems in the calibration of multiple scan fields,a novel calibration system is designed in this study to realize in situ auto-detection of numerous laser spots in the build chamber to ensure high efficiency and accuracy.Moreover,because the detectable area could not cover the entire build area and the detection data still contained errors,a virtual laser-scanner system was established by identifying the assembly defects and galvo nonlinearities of the ML-PBF system from the detection data,which served as the system's controller to improve calibration accuracy.The multi-field alignment error was less than 0.012%,which could avoid the intersection and separation of scan paths in multi-laser scanning and therefore meet the requirements for high-precision ML-PBF.Finally,the reliability of the method was verified theoretically using principal component analysis.
基金supported by the National Natural Science Foundation of China (51475353, 51475352 and 51375361)the Tribology Science Fund of the State Key Laboratory of Tribology of China (SKLTKF14A02)