The mercury-antimony-gold ore was subjected of the flotation. As a result of enrichment of ore, the mercury-antimony concentrate with the contents of 51.5% Sb, 3.55% Hg and 6 g/t Au was received. Vacuum distillation o...The mercury-antimony-gold ore was subjected of the flotation. As a result of enrichment of ore, the mercury-antimony concentrate with the contents of 51.5% Sb, 3.55% Hg and 6 g/t Au was received. Vacuum distillation of concentrate allocation in serial sublimates mercury and antimony was designed. The big amount gold passed to calcine after vacuum distillation. The gold in calcine roastin uo to 900 ℃was 30.6 e/t.展开更多
Dimethylsulfoxide(DMSO)extraction is commonly used to study the chemical structures of orig-inal xylan in the plant cell wall,since the DMSO can preserve the original structure of the xylan as much as possible during ...Dimethylsulfoxide(DMSO)extraction is commonly used to study the chemical structures of orig-inal xylan in the plant cell wall,since the DMSO can preserve the original structure of the xylan as much as possible during the extracting process.In addition,the DMSO-extracted xylans have unique properties allowing their potential applications in emulsifying or filming materials.How-ever,the yield of DMSO-extracted xylan is always low and the effects of different DMSO extraction conditions on the chemical compositions of xylan have not been fully studied,which greatly hin-ders its researches and applications.In this study,we have found that extensive delignification before DMSO extraction results in destruction of lignin-carbohydrate complex(LCC),leading to xylan yield and xylose unit content increased by up to 220%and 20%,respectively.Tert-butanol washing of the holocellulose can further increase the DMSO extracted xylan yield by∼10%.The yield of xylan extracted by the DMSO at 80°C for 7 h was obviously higher than that at room temperature for 3 d by 30%-40%.Thermal analysis showed that the xylans extracted at differ-ent conditions had thermal stability without obvious differences.The results indicate that the DMSO-extracted xylan with a high yield,a high purity and a high degree of acetylation can be ex-tracted at a high delignification level,a high reaction temperature and a short reaction time.This study is of great significance for studying xylan structure-property relationships and promoting the applications of DMSO-extracted xylan.展开更多
文摘The mercury-antimony-gold ore was subjected of the flotation. As a result of enrichment of ore, the mercury-antimony concentrate with the contents of 51.5% Sb, 3.55% Hg and 6 g/t Au was received. Vacuum distillation of concentrate allocation in serial sublimates mercury and antimony was designed. The big amount gold passed to calcine after vacuum distillation. The gold in calcine roastin uo to 900 ℃was 30.6 e/t.
基金supported by Natural Science Foundation of Guangdong Province(No.2020A1515011021).
文摘Dimethylsulfoxide(DMSO)extraction is commonly used to study the chemical structures of orig-inal xylan in the plant cell wall,since the DMSO can preserve the original structure of the xylan as much as possible during the extracting process.In addition,the DMSO-extracted xylans have unique properties allowing their potential applications in emulsifying or filming materials.How-ever,the yield of DMSO-extracted xylan is always low and the effects of different DMSO extraction conditions on the chemical compositions of xylan have not been fully studied,which greatly hin-ders its researches and applications.In this study,we have found that extensive delignification before DMSO extraction results in destruction of lignin-carbohydrate complex(LCC),leading to xylan yield and xylose unit content increased by up to 220%and 20%,respectively.Tert-butanol washing of the holocellulose can further increase the DMSO extracted xylan yield by∼10%.The yield of xylan extracted by the DMSO at 80°C for 7 h was obviously higher than that at room temperature for 3 d by 30%-40%.Thermal analysis showed that the xylans extracted at differ-ent conditions had thermal stability without obvious differences.The results indicate that the DMSO-extracted xylan with a high yield,a high purity and a high degree of acetylation can be ex-tracted at a high delignification level,a high reaction temperature and a short reaction time.This study is of great significance for studying xylan structure-property relationships and promoting the applications of DMSO-extracted xylan.
